(+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol

Base Information

Chemical Name:(+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol
CAS No.:702684-35-3
Molecular Formula:C₁₇H₁₉NO₂
Molecular Weight:269.343
Hs Code.:

Synonyms:(+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol

Chemical Property:

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Technology Process of (+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol

There total 1 articles about (+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 54884-55-8
2-methoxy-6-methyl-benzaldehyde

: 20989-17-7
(2S)-2-phenylglycinol

: 702684-35-3
(+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol

Guidance literature:: With 4A MS; In ethanol; at 20 ℃; for 26h;
DOI:10.1002/hlca.200490054

Reference yield: 67.0%

: 917-54-4
methyllithium

: 702684-35-3
(+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol

: 702684-36-4
(+)-(βS)-β-{[(1S)-1-(2-methoxy-6-methylphenyl)ethyl]amino}benzeneethanol

Guidance literature:: In tetrahydrofuran; diethyl ether; at -78 ℃; for 48h;
DOI:10.1002/hlca.200490054

Reference yield:

: 702684-35-3
(+)-(βS)-β-{[(1E)-(2-methoxy-6-methylphenyl)methylene]amino}benzeneethanol

: 702684-37-5
(-)-[(1S)-1-(2-methoxy-6-methylphenyl)ethyl]amine

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / tetrahydrofuran; diethyl ether / 48 h / -78 °C

2: 5.30 g / K₂CO₃; Pb(OAc)4 / methanol; CH₂Cl₂ / 0 °C

3: 2.38 g / aq. HCl / CH₂Cl₂ / 15 h / 20 °C

With lead(IV) acetate; hydrogenchloride; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;
DOI:10.1002/hlca.200490054