dichlorobis(triphenylphosphine)nitridotechnetium(V)

Base Information

Chemical Name:dichlorobis(triphenylphosphine)nitridotechnetium(V)
CAS No.:113945-92-9
Molecular Formula:C₃₆H₃₀Cl₂NP₂Tc
Molecular Weight:708.494
Hs Code.:

Synonyms:dichlorobis(triphenylphosphine)nitridotechnetium(V)

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Chemical Property of dichlorobis(triphenylphosphine)nitridotechnetium(V)

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Technology Process of dichlorobis(triphenylphosphine)nitridotechnetium(V)

There total 5 articles about dichlorobis(triphenylphosphine)nitridotechnetium(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 114368-22-8
chlorotetrakis(thiourea)nitridotechnetium(V)

: 113945-92-9
dichlorobis(triphenylphosphine)nitridotechnetium(V)

Guidance literature:: With PPh₃; In ethanol; water; Tc complex dissolved in H2O/EtOH; PPh3 dissolved in ethanol, refluxed for 5 min, pptn.,; filtration, ppt. washed with hot EtOH and dried;
DOI:10.1016/S0020-1693(00)83898-0

Reference yield: 90.0%

: 95012-25-2
[As(C₆H₅)4][(99g)Tc(N)Cl₄]

: 603-35-0
triphenylphosphine

: 113945-92-9
dichlorobis(triphenylphosphine)nitridotechnetium(V)

Guidance literature:: With PPh₃; In acetonitrile; AsPh4(TcNCl4) is dissolved in MeCN and then is added a soln. of PPh3 inMeCN; ppt. is collected by filtn., washed with MeCN and dried;

Reference yield:

: ammonium [⁽⁹⁹⁾Tc]pertechnate

: 5397-03-5
hydrazinecarbodithioic acid methyl ester

: 113945-92-9
dichlorobis(triphenylphosphine)nitridotechnetium(V)

Guidance literature:: With triphenylphosphine; In ethanol; ethanolic soln. of ligand was added at room temp. to a stirred soln. of pertechnetate followed by HCl, PPh3 dissolved in hot EtOH was added, mixt. was stirred for 15 min at room temp.;; ppt. was filtered off and washed with hot ethanol, acetone and Et2O; elem. anal.;