(S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol

Base Information

Chemical Name:(S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol
CAS No.:369375-76-8
Molecular Formula:C₁₈H₂₈O₄
Molecular Weight:308.418
Hs Code.:

Synonyms:(S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol

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Chemical Property of (S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol

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Technology Process of (S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol

There total 1 articles about (S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: (S)-4-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-2,2-dimethyl-[1,3]dioxolane

: 369375-76-8
(S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol

Guidance literature:: With toluene-4-sulfonic acid; In methanol;
DOI:10.1016/S0957-4166(01)00244-0

Reference yield: 90.0%

: 98-59-9
p-toluenesulfonyl chloride

: 369375-76-8
(S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol

: 369375-78-0
Toluene-4-sulfonic acid (S)-2-((2S,4S,5S)-4-benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-2-hydroxy-ethyl ester

Guidance literature:: With di(n-butyl)tin oxide; triethylamine; In dichloromethane;
DOI:10.1016/S0957-4166(01)00244-0

Reference yield:

: 369375-76-8
(S)-1-((2S,4S,5S)-4-Benzyloxy-5-pentyl-tetrahydro-furan-2-yl)-ethane-1,2-diol

: 287483-50-5
tert-butyl-[5-((2S)-oxiran-2-yl)-2-(2S,3S,5S)-2-pentyltetrahydrofuran-3-yloxy]-diphenylsilane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / Bu₂SnO; Et₃N / CH₂Cl₂

2: 90 percent / K₂CO₃ / methanol

3: 87 percent / HCOOH / Pd (black) / methanol

4: 100 percent / imidazole / CH₂Cl₂

With 1H-imidazole; formic acid; di(n-butyl)tin oxide; potassium carbonate; triethylamine; palladium; In methanol; dichloromethane;
DOI:10.1016/S0957-4166(01)00244-0