5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole

Base Information

Chemical Name:5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole
CAS No.:908370-02-5
Molecular Formula:C₂₉H₃₆N₄O₃SSi
Molecular Weight:548.781
Hs Code.:

5-[5-(<i>tert</i>-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1<i>H</i>-tetrazole

Synonyms:5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole

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Chemical Property of 5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole

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Technology Process of 5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole

There total 5 articles about 5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 121671-81-6
(S)-5-(tert-butyldiphenylsilyloxy)hexan-1-ol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 908370-02-5
5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole

Guidance literature:: (S)-5-(tert-butyldiphenylsilyloxy)hexan-1-ol; 1-Phenyl-1H-tetrazole-5-thiol; With di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

With ammonium molybdate; dihydrogen peroxide; In ethanol; at 20 ℃; for 0.25h; Ionic liquid;
DOI:10.1039/c2ob26533h

Reference yield:

: 5-[5-(tert-butyl-diphenyl-silanyloxy)-hexylsulfanyl]-1-phenyl-1H-tetrazole

: 908370-02-5
5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole

Guidance literature:: With ammonium heptamolybdate; dihydrogen peroxide; In ethanol; at 20 ℃;
DOI:10.1055/s-2006-941575

Reference yield:

: 345653-64-7
(S)-tert-butyl(hex-5-en-2-yloxy)diphenylsilane

: 908370-02-5
5-[5-(tert-butyl-diphenyl-silanyloxy)-hexane-1-sulfonyl]-1-phenyl-1H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 6 h / 20 °C / Inert atmosphere

1.2: 4 h / 20 °C / Inert atmosphere

2.1: triphenylphosphine; toluene-4-sulfonic acid; di-isopropyl azodicarboxylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.2: 0.25 h / 20 °C / Ionic liquid

With di-isopropyl azodicarboxylate; dimethylsulfide borane complex; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran;
DOI:10.1039/c2ob26533h