N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea

Base Information

Chemical Name:N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea
CAS No.:118576-40-2
Molecular Formula:C₁₅H₁₆F₆N₂O₃
Molecular Weight:386.294
Hs Code.:

Synonyms:N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea

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Chemical Property of N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea

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Technology Process of N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea

There total 6 articles about N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: <2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>carbamoyl azide

: 62-53-3
aniline

: 118576-40-2
N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea

Guidance literature:: In 1,4-dioxane; water; acetone; at 100 ℃; for 5h;
DOI:10.1021/jo00265a029

Reference yield:

: 53392-81-7
dimethyl 2,3-bis-(2,2,2-trifluoroethyl)succinate

: 118576-40-2
N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea

Guidance literature:: Multi-step reaction with 5 steps

1: 20 percent / 35percent aq. HCl, acetic acid / 8 h / 100 °C

2: SOCl₂ / CH₂Cl₂ / 2 h / Heating

3: NaN₃ / acetone; H₂O

4: acetone; H₂O / 24 h / Ambient temperature

5: 91 percent / dioxane; acetone; H₂O / 5 h / 100 °C

With hydrogenchloride; thionyl chloride; sodium azide; acetic acid; In 1,4-dioxane; dichloromethane; water; acetone;
DOI:10.1021/jo00265a029

Reference yield:

: 3-Chlorocarbonyl-5,5,5-trifluoro-2-(2,2,2-trifluoro-ethyl)-pentanoic acid methyl ester

: 118576-40-2
N-<2-(methoxycarbonyl)-4,4,4-trifluoro-1-(2,2,2-trifluoroethyl)butyl>-N'-phenylurea

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / acetone; H₂O

2: acetone; H₂O / 24 h / Ambient temperature

3: 91 percent / dioxane; acetone; H₂O / 5 h / 100 °C

With sodium azide; In 1,4-dioxane; water; acetone;
DOI:10.1021/jo00265a029