C₂₃H₂₂F₃NO₅SSe

Base Information

Chemical Name:C₂₃H₂₂F₃NO₅SSe
CAS No.:1332497-95-6
Molecular Formula:C₂₃H₂₂F₃NO₅SSe
Molecular Weight:560.453
Hs Code.:

C<sub>23</sub>H<sub>22</sub>F<sub>3</sub>NO<sub>5</sub>SSe

Synonyms:C₂₃H₂₂F₃NO₅SSe

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Chemical Property of C₂₃H₂₂F₃NO₅SSe

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Technology Process of C₂₃H₂₂F₃NO₅SSe

There total 7 articles about C₂₃H₂₂F₃NO₅SSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1332494-98-0
C₂₃H₂₂F₃NO₃SSe

: 1332497-95-6
C₂₃H₂₂F₃NO₅SSe

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 5 ℃; for 2h;

Reference yield:

: 1332497-98-9
4-(trifluoromethyl)benzoselenoamide

: 1332497-95-6
C₂₃H₂₂F₃NO₅SSe

Guidance literature:: Multi-step reaction with 6 steps

1.1: tetrahydrofuran / 12.83 h / 20 - 80 °C / Reflux

1.2: 0.33 h / 20 °C

2.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere

3.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 1 h / 20 °C

4.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C

4.2: 0.17 h / -78 °C

5.1: potassium carbonate / water; acetone / 4 h / 20 °C

6.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 5 °C

With N-chloro-succinimide; isopropylmagnesium chloride; diisobutylaluminium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; water; acetone;

Reference yield:

: 455-18-5
4-CF₃C₆H₄CN

: 1332497-95-6
C₂₃H₂₂F₃NO₅SSe

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogenchloride; pyridine / ethanol / 2 h / Inert atmosphere; Reflux

2.1: tetrahydrofuran / 12.83 h / 20 - 80 °C / Reflux

2.2: 0.33 h / 20 °C

3.1: diisobutylaluminium hydride / dichloromethane; hexane / 1.5 h / -78 - -10 °C / Inert atmosphere

4.1: N-chloro-succinimide; triphenylphosphine / dichloromethane / 1 h / 20 °C

5.1: isopropylmagnesium chloride / tetrahydrofuran / 0.17 h / 0 °C

5.2: 0.17 h / -78 °C

6.1: potassium carbonate / water; acetone / 4 h / 20 °C

7.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 0 - 5 °C

With pyridine; hydrogenchloride; N-chloro-succinimide; isopropylmagnesium chloride; diisobutylaluminium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; acetone;