C₄₃H₇₅NO₁₁Si

Base Information

Chemical Name:C₄₃H₇₅NO₁₁Si
CAS No.:922166-95-8
Molecular Formula:C₄₃H₇₅NO₁₁Si
Molecular Weight:810.154
Hs Code.:

C<sub>43</sub>H<sub>75</sub>NO<sub>11</sub>Si

Synonyms:C₄₃H₇₅NO₁₁Si

Suppliers and Price of C₄₃H₇₅NO₁₁Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₃H₇₅NO₁₁Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₃H₇₅NO₁₁Si

There total 25 articles about C₄₃H₇₅NO₁₁Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 922166-84-5
(E)-N-{3-[(1R,2S,4S,5R,6S,9S,10S)-9-tert-butyldimethylsilyloxy-1,4,5,10-tetramethoxy-2,6,8-trimethyldodec-7,11-dienyl]-2,5-dimethoxyphenyl}amine

: 24424-99-5
di-tert-butyl dicarbonate

: 922166-95-8
C₄₃H₇₅NO₁₁Si

Guidance literature:: With dmap; triethylamine; In tetrahydrofuran; for 6h; Heating;
DOI:10.1021/ol062642i

Reference yield:

: 922166-82-3
N,N-diallyl-3-bromo-2,5-dimethoxyaniline

: 922166-95-8
C₄₃H₇₅NO₁₁Si

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / n-BuLi / diethyl ether; hexane / 1.5 h / -78 °C

2: 100 percent / NaH / dimethylformamide / 0 - 20 °C

3: 97 percent / N,N-dimethylbarbituric acid; Pd(PPh₃)4 / CH₂Cl₂ / 2.5 h / Heating

4: 75 percent / Et₃N; N,N-dimethylaminopyridine / tetrahydrofuran / 6 h / Heating

With dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 1,3-dimethylbarbituric acid; sodium hydride; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol062642i

Reference yield:

: tert-butyl-(4-methoxy-2-methyl-but-3-enyloxy)-diphenyl-silane

: 922166-95-8
C₄₃H₇₅NO₁₁Si

Guidance literature:: Multi-step reaction with 19 steps

1.1: 4.37 mg / aq. HCl / tetrahydrofuran; CH₂Cl₂ / 3 h / 20 °C

2.1: 96 percent / (S,S)-chiral titanium complex / diethyl ether; tetrahydrofuran / 5 h / -78 °C

3.1: 97 percent / KH / tetrahydrofuran / 0 - 20 °C

4.1: 98 percent / [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; N-allyl-N-tritylamine; diisopropylethylamine / toluene / 3.5 h / Heating

5.1: OsO₄; H₂O; N-methylmorpholine N-oxide / acetone / 16 h / 20 °C

6.1: aq. NaIO₄ / acetone / 2.5 h / 20 °C

7.1: 2.73 g / 4 Angstroem molecular sieves / toluene / 2.5 h / -78 - 0 °C

8.1: 92 percent / KH / tetrahydrofuran / 0 - 20 °C

9.1: OsO₄; H₂O; N-methylmorpholine N-oxide / acetone / 18 h / 20 °C

10.1: aq. NaIO₄ / acetone / 2.5 h / 20 °C

11.1: s-BuLi / tetrahydrofuran; cyclohexane / 4.5 h / -78 - -20 °C

11.2: 1.18 g / citric acid / tetrahydrofuran; cyclohexane; H₂O / pH 4 - 5

12.1: BF₃*Et₂O / tetrahydrofuran; cyclohexane / -78 - -5 °C

12.2: 1.49 g / ethanolamine / pentane / 2.5 h / 0 °C

13.1: 94 percent / 2,6-lutidine / CH₂Cl₂ / 10 h / -78 °C

14.1: 82 percent / NH₄F; MeOH / 9.5 h / Heating

15.1: Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 4 h

16.1: 54 percent / n-BuLi / diethyl ether; hexane / 1.5 h / -78 °C

17.1: 100 percent / NaH / dimethylformamide / 0 - 20 °C

18.1: 97 percent / N,N-dimethylbarbituric acid; Pd(PPh₃)4 / CH₂Cl₂ / 2.5 h / Heating

19.1: 75 percent / Et₃N; N,N-dimethylaminopyridine / tetrahydrofuran / 6 h / Heating

With 2,6-dimethylpyridine; hydrogenchloride; methanol; dmap; ammonium fluoride; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; 1,3-dimethylbarbituric acid; (S,S)-chiral titanium; [1,3-Mes₂-(N₂C₃H₅)]Cl₂(PCy₃)Ru=CHPh; 4 A molecular sieve; boron trifluoride diethyl etherate; N-tritylprop-2-en-1-amine; water; sec.-butyllithium; potassium hydride; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; cyclohexane; N,N-dimethyl-formamide; acetone; toluene; 11.1: Corey-Schlessinger olefination / 15.1: Dess-Martin oxidation;
DOI:10.1021/ol062642i