di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate

Base Information

Chemical Name:di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate
CAS No.:848134-45-2
Molecular Formula:C₂₇H₂₈ClN₅O₇
Molecular Weight:570.002
Hs Code.:

Synonyms:di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate

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Chemical Property of di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate

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Technology Process of di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate

There total 4 articles about di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 214470-33-4
4-chloro-7-methoxy-6-nitro-quinoline-3-carbonitrile

: 252019-51-5
N¹,N¹-bis(tert-butoxycarbonyl)-2-chloro-p-phenylenediamine

: 848134-45-2
di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate

Guidance literature:: In isopropyl alcohol; for 1h; Heating;
DOI:10.1021/jm040159c

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 848134-45-2
di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / DMAP / tetrahydrofuran / 3 h / 25 °C

2: 100 percent / iron; AcOH / methanol / 0.5 h / Heating

3: 90 percent / propan-2-ol / 1 h / Heating

With dmap; iron; acetic acid; In tetrahydrofuran; methanol; isopropyl alcohol;
DOI:10.1021/jm040159c

Reference yield:

: 121-87-9
2-Chloro-4-nitroaniline

: 848134-45-2
di(tert-butyl)-2-chloro-4-[(3-cyano-7-methoxy-6-nitro-4-quinolinyl)amino]phenylimidodicarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / DMAP / tetrahydrofuran / 3 h / 25 °C

2: 100 percent / iron; AcOH / methanol / 0.5 h / Heating

3: 90 percent / propan-2-ol / 1 h / Heating

With dmap; iron; acetic acid; In tetrahydrofuran; methanol; isopropyl alcohol;
DOI:10.1021/jm040159c