(4S)-4-[(1S)-2-azido-1-(4-t-butylbenzyl)ethyl]-2,2-dimethyl-1,3-dioxolane

Base Information

Chemical Name:(4S)-4-[(1S)-2-azido-1-(4-t-butylbenzyl)ethyl]-2,2-dimethyl-1,3-dioxolane
CAS No.:1003002-80-9
Molecular Formula:C₁₈H₂₇N₃O₂
Molecular Weight:317.431
Hs Code.:

Synonyms:(4S)-4-[(1S)-2-azido-1-(4-t-butylbenzyl)ethyl]-2,2-dimethyl-1,3-dioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-4-[(1S)-2-azido-1-(4-t-butylbenzyl)ethyl]-2,2-dimethyl-1,3-dioxolane

Chemical Property:

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Technology Process of (4S)-4-[(1S)-2-azido-1-(4-t-butylbenzyl)ethyl]-2,2-dimethyl-1,3-dioxolane

There total 2 articles about (4S)-4-[(1S)-2-azido-1-(4-t-butylbenzyl)ethyl]-2,2-dimethyl-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18880-00-7
1-(bromomethyl)-4-(1,1-dimethylethyl)benzene

: 1003002-80-9
(4S)-4-[(1S)-2-azido-1-(4-t-butylbenzyl)ethyl]-2,2-dimethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: lithium hexamethyldisilazane; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran

2: triphenylphosphine; diphenyl phosphoryl azide; diethylazodicarboxylate / tetrahydrofuran

With N,N,N,N,N,N-hexamethylphosphoric triamide; diphenyl phosphoryl azide; triphenylphosphine; lithium hexamethyldisilazane; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2014.04.054

Reference yield:

: C₁₅H₂₄O₅

: 1003002-80-9
(4S)-4-[(1S)-2-azido-1-(4-t-butylbenzyl)ethyl]-2,2-dimethyl-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid

2: triphenylphosphine; diethylazodicarboxylate; diphenyl phosphoryl azide / tetrahydrofuran

With diphenyl phosphoryl azide; toluene-4-sulfonic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2014.04.054