(2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone

Base Information

Chemical Name:(2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone
CAS No.:76192-81-9
Molecular Formula:C₂₅H₃₂O₃
Molecular Weight:380.527
Hs Code.:

Synonyms:(2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone

Suppliers and Price of (2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of (2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone

There total 2 articles about (2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 76207-98-2
(1S,3S,6R)-3-Benzyloxymethyl-3,7,7-trimethyl-bicyclo[4.1.0]heptan-2-one

: 100-51-6,185532-71-2
benzyl alcohol

: 76192-81-9
(2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone

Guidance literature:: With toluene-4-sulfonic acid;
DOI:10.1021/ja00545a032

Reference yield:

: 497-62-1,5561-14-8,16838-46-3,16838-48-5,18541-52-1,24563-23-3,57693-89-7,74431-68-8,83945-86-2,85993-62-0
(-)-2-carone

: 76192-81-9
(2S,5R)-2-Benzyloxymethyl-5-(1-benzyloxy-1-methyl-ethyl)-2-methyl-cyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / LDA / tetrahydrofuran

2: 85 percent / p-toluenesulfonic acid

With toluene-4-sulfonic acid; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja00545a032