benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

Base Information

Chemical Name:benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside
CAS No.:1056476-10-8
Molecular Formula:C₈₇H₁₀₀O₁₆Si
Molecular Weight:1429.83
Hs Code.:

benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

Synonyms:benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

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Chemical Property of benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

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Technology Process of benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

There total 1 articles about benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1056476-06-2
benzyl (2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

: 1056476-10-8
benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

Guidance literature:: With sodium methylate; In methanol;
DOI:10.1073/pnas.1002717107

Reference yield: 47.0%

: 1056476-10-8
benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

: 38184-10-0,62774-37-2,74801-29-9,91602-61-8,116501-52-1,139974-84-8,116501-53-2
phenyl 2,3,4,6-tetra-O-benzyl-1-thio-α-D-mannopyranoside

: benzyl 2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

Guidance literature:: benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside; phenyl 2,3,4,6-tetra-O-benzyl-1-thio-α-D-mannopyranoside; With 2,6-di-tert-butyl-4-methylpyridine; In dichloromethane; for 1h; Molecular sieve;

With Dimethyldisulphide; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1039/b803999m

Reference yield:

: 1056476-10-8
benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

: 38184-10-0,62774-37-2,74801-29-9,91602-61-8,116501-52-1,139974-84-8,116501-53-2
phenyl 2,3,4,6-tetra-O-benzyl-1-thio-α-D-mannopyranoside

: benzyl 2,3,4,6-tetra-O-benzyl-β-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

: benzyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl-(1>2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->2)-3,4,6-tri-O-benzyl-α-D-mannopyranosyl-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside

Guidance literature:: benzyl (3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-α-D-mannopyranoside; phenyl 2,3,4,6-tetra-O-benzyl-1-thio-α-D-mannopyranoside; With 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; for 1h; Molecular sieve;

With dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In dichloromethane; at -78 ℃; for 1h; optical yield given as %de; Inert atmosphere;
DOI:10.1039/b803999m