C₆₀H₁₁₃ClO₁₂Si₄

Base Information

Chemical Name:C₆₀H₁₁₃ClO₁₂Si₄
CAS No.:1032989-75-5
Molecular Formula:C₆₀H₁₁₃ClO₁₂Si₄
Molecular Weight:1174.35
Hs Code.:

C<sub>60</sub>H<sub>113</sub>ClO<sub>12</sub>Si<sub>4</sub>

Synonyms:C₆₀H₁₁₃ClO₁₂Si₄

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Chemical Property of C₆₀H₁₁₃ClO₁₂Si₄

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Technology Process of C₆₀H₁₁₃ClO₁₂Si₄

There total 10 articles about C₆₀H₁₁₃ClO₁₂Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1032989-96-0
C₆₀H₁₁₅ClO₁₂Si₄

: 1032989-75-5
C₆₀H₁₁₃ClO₁₂Si₄

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane;
DOI:10.1002/anie.200705565

Reference yield:

: C₂₉H₅₇ClO₇Si₂

: 1032989-75-5
C₆₀H₁₁₃ClO₁₂Si₄

Guidance literature:: Multi-step reaction with 9 steps

1: 1H-imidazole / dichloromethane / 0.17 h / Inert atmosphere

2: pyridinium p-toluenesulfonate / methane; dichloromethane / 1.5 h / 0 °C / Inert atmosphere

3: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / Inert atmosphere

4: tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C / Inert atmosphere

5: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / Inert atmosphere

6: dimethyl sulfide borane / tetrahydrofuran / 2 h / Inert atmosphere

7: 2,6-dimethylpyridine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

8: pyridinium p-toluenesulfonate / methanol; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

9: dmap; sodium hydrogencarbonate / dicholromethane / 1 h / Inert atmosphere

With 1H-imidazole; 2,6-dimethylpyridine; dmap; dimethyl sulfide borane; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; Dess-Martin periodane; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; methanol; dicholromethane; methane; hexane; dichloromethane; 3: Dess-Martin oxidation / 4: Wittig olefination;
DOI:10.1039/c2ob25101a

Reference yield:

: C₂₉H₅₅ClO₇Si₂

: 1032989-75-5
C₆₀H₁₁₃ClO₁₂Si₄

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran; hexane / 0.5 h / -78 - 20 °C / Inert atmosphere

2: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / Inert atmosphere

3: dimethyl sulfide borane / tetrahydrofuran / 2 h / Inert atmosphere

4: 2,6-dimethylpyridine / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

5: pyridinium p-toluenesulfonate / methanol; dichloromethane / 0.5 h / 0 °C / Inert atmosphere

6: dmap; sodium hydrogencarbonate / dicholromethane / 1 h / Inert atmosphere

With 2,6-dimethylpyridine; dmap; dimethyl sulfide borane; pyridinium p-toluenesulfonate; sodium hydrogencarbonate; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; methanol; dicholromethane; hexane; dichloromethane; 1: Wittig olefination;
DOI:10.1039/c2ob25101a