4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid

Base Information

Chemical Name:4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid
CAS No.:847237-15-4
Molecular Formula:C₄₈H₃₂Cl₂O₆
Molecular Weight:775.684
Hs Code.:

Synonyms:4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid

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Chemical Property of 4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid

Chemical Property:

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Technology Process of 4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid

There total 3 articles about 4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 847237-15-4
4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / CsF / Pd(PPh₃)4 / 1,2-dimethoxy-ethane / 48 h / Heating

2: NaOH / tetrahydrofuran; methanol; H₂O / 20 °C

With sodium hydroxide; cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; 1: Suzuki coupling;
DOI:10.1002/anie.200461214

Reference yield:

: C₅₀H₃₆Cl₂O₆

: 847237-15-4
4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid

Guidance literature:: With sodium hydroxide; In tetrahydrofuran; methanol; water; at 20 ℃;
DOI:10.1002/anie.200461214

Reference yield:

: 431043-67-3,431043-69-5
4,4'-dibromo-6,6'-dichloro-2,2'-dibenzyloxy-1,1'-binaphthalene

: 847237-15-4
4,4'-[6,6'-dichloro-2,2'-di(benzyloxy)-1,1'-binaphthalene-4,4'-diyl]dibenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / CsF / Pd(PPh₃)4 / 1,2-dimethoxy-ethane / 48 h / Heating

2: NaOH / tetrahydrofuran; methanol; H₂O / 20 °C

With sodium hydroxide; cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; 1: Suzuki coupling;
DOI:10.1002/anie.200461214