4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

Base Information

Chemical Name:4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one
CAS No.:160409-45-0
Molecular Formula:C₃₉H₄₆O₃S₄Si₂
Molecular Weight:747.227
Hs Code.:

Synonyms:4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

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Chemical Property of 4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

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Technology Process of 4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

There total 3 articles about 4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 160409-44-9
4,5-bis<2-(tert-butyldiphenylsilyloxy)ethylthio>-1,3-dithiole-2-thione

: 160409-45-0
4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

Guidance literature:: With mercury(II) diacetate; In chloroform; acetic acid; at 20 ℃; for 16h;
DOI:10.1055/s-1994-25606

Reference yield:

: 128258-71-9
4,5-bis[(2'-hydroxyethyl)thio]1,3-dithiole-2-thione

: 160409-45-0
4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / imidazole / dimethylformamide / 16 h / 20 °C

2: 100 percent / Hg(OAc)2 / acetic acid; CHCl₃ / 16 h / 20 °C

With 1H-imidazole; mercury(II) diacetate; In chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1055/s-1994-25606

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 160409-45-0
4,5-Bis-[2-(tert-butyl-diphenyl-silanyloxy)-ethylsulfanyl]-[1,3]dithiol-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / imidazole / dimethylformamide / 16 h / 20 °C

2: 100 percent / Hg(OAc)2 / acetic acid; CHCl₃ / 16 h / 20 °C

With 1H-imidazole; mercury(II) diacetate; In chloroform; acetic acid; N,N-dimethyl-formamide;
DOI:10.1055/s-1994-25606