2-iodo-N,N-diallylaniline

Base Information

• Chemical Name: 2-iodo-N,N-diallylaniline
• CAS No.: 73396-92-6
• Molecular Formula: C₁₂H₁₄IN
• Molecular Weight: 299.154
• Mol file: 73396-92-6.mol

Synonyms:2-iodo-N,N-diallylaniline

Chemical Property of 2-iodo-N,N-diallylaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-iodo-N,N-diallylaniline

There total 4 articles about 2-iodo-N,N-diallylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-iodophenylamine (615-43-0) + allyl bromide (106-95-6) → 2-iodo-N,N-diallylaniline (73396-92-6)

Guidance literature:

2-iodophenylamine; With cetyltrimethylammonim bromide; sodium carbonate; In N,N-dimethyl-formamide; for 0.0833333h;

allyl bromide; In N,N-dimethyl-formamide; at 130 ℃; for 0.333333h; Microwave irradiation;

DOI:10.1016/j.tetlet.2014.03.044

Reference yield: 85.0%

2-iodophenylamine (615-43-0) + allyl bromide (106-95-6) → 2-iodo-N-allylaniline (73396-87-9) + 2-iodo-N,N-diallylaniline (73396-92-6)

Guidance literature:

With silica gel; at 20 ℃; for 10h;

DOI:10.1039/b905878h

Reference yield:

2-iodophenylamine (615-43-0) → 2-iodo-N,N-diallylaniline (73396-92-6)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

2: 1) NaH / 1) DMF, 0 deg C, 1 h, 2) warming up to room temperature

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jo00312a025

upstream raw materials:

2-iodo-N-allylaniline

allyl bromide

2-iodophenylamine

Downstream raw materials:

N-allyl-3-((1-hydroxycyclohexyl)methyl)indoline

N,N-diallylaniline

1-allyl-3-methyl-2,3-dihydro-1H-indole

N-allyl-3-methylindole