tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate

Base Information

Chemical Name:tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate
CAS No.:867150-96-7
Molecular Formula:C₃₃H₅₅ClO₃S
Molecular Weight:567.317
Hs Code.:

Synonyms:tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate

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Chemical Property of tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate

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Technology Process of tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate

There total 1 articles about tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: [Chloro-((R)-toluene-4-sulfinyl)-methylene]-cyclopentadecane

: 2492-18-4
tert-butyl hexanoate

: 867150-96-7
tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate

Guidance literature:: tert-butyl hexanoate; With lithium diisopropyl amide; In tetrahydrofuran; at -75 ℃;

[Chloro-((R)-toluene-4-sulfinyl)-methylene]-cyclopentadecane; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.06.172

Reference yield: 82.0%

: 867150-96-7
tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate

: 867151-03-9
(R)-2-[1-((S)-Toluene-4-sulfinylmethyl)-cyclopentadecyl]-hexanoic acid tert-butyl ester

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;
DOI:10.1016/j.tetlet.2005.06.172

Reference yield:

: 867150-96-7
tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}hexanoate

: (2R)-(-)-tert-butyl 2-{1-[(p-tolylsulfonyl)methyl]cyclopentadecyl}hexanoate

Guidance literature:: Multi-step reaction with 2 steps

1: Bu₃SnH; AIBN / benzene / Heating

2: m-CPBA / CH₂Cl₂ / 20 °C

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene;
DOI:10.1016/j.tetasy.2007.07.033