furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide

Base Information

Chemical Name:furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide
CAS No.:1445796-99-5
Molecular Formula:C₂₆H₂₈N₂O₅
Molecular Weight:448.519
Hs Code.:

Synonyms:furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide

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Technology Process of furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide

There total 3 articles about furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 440087-51-4
1-[4-(4-methoxyphenyl)tetrahydro-2H-pyran-4-yl]-methylamine

: 1445797-09-0
C₁₄H₁₃NO₄

: 1445796-99-5
furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide

Guidance literature:: With trimethylaluminum; In toluene; Reflux;

Reference yield:

: 619-45-4
4-methoxycarbonyl aniline

: 1445796-99-5
furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dichloromethane / 20 °C

2.1: sodium hydride; N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 16 h / 20 °C

3.1: trimethylaluminum / toluene / Reflux

With trimethylaluminum; sodium hydride; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; toluene;

Reference yield:

: 527-69-5
2-furancarbonyl chloride

: 1445796-99-5
furan-2-carboxylic acid (4-{[4-(4-methoxyphenyl)tetrahydropyran-4-ylmethyl]carbamoyl}phenyl)methylamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dichloromethane / 20 °C

2.1: sodium hydride; N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 16 h / 20 °C

3.1: trimethylaluminum / toluene / Reflux

With trimethylaluminum; sodium hydride; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; toluene;