[(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine

Base Information

Chemical Name:[(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine
CAS No.:876314-17-9
Molecular Formula:C₂₆H₃₃NO₆S
Molecular Weight:487.617
Hs Code.:

Synonyms:[(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine

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Chemical Property of [(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine

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Technology Process of [(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine

There total 1 articles about [(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 100777-91-1
(2S)-2,3-O-isopropylideneglyceraldehyde N-benzylimine

: 527729-45-9
(-)-(1R,2S)-2-(2-benzenesulfonylvinyl)-1-methoxymethoxy-cyclopropane

: 876314-19-1
(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-propylamine

: 876314-17-9
[(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine

Guidance literature:: (-)-(1R,2S)-2-(2-benzenesulfonylvinyl)-1-methoxymethoxy-cyclopropane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.25h;

(2S)-2,3-O-isopropylideneglyceraldehyde N-benzylimine; In tetrahydrofuran; at -78 ℃; for 1h;
DOI:10.1055/s-2005-870005

Reference yield: 28.0%

: 876314-17-9
[(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine

: 876314-19-1
(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-propylamine

: [(1S,2R)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-propyl]-[1-phenyl-meth-(E)-ylidene]-amine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 - 0 ℃; for 7h;
DOI:10.1055/s-2005-870005

Reference yield:

: 876314-17-9
[(E)-(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-allyl]-benzyl-amine

: 876314-20-4
[(S)-2-Benzenesulfonyl-1-((S)-2,2-dimethyl-[1,3]dioxolan-4-yl)-3-((1S,2R)-2-methoxymethoxy-cyclopropyl)-propyl]-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / BuLi / tetrahydrofuran / 7 h / -78 - 0 °C

2: 76 percent / tetrahydrofuran / 16 h

With n-butyllithium; In tetrahydrofuran;
DOI:10.1055/s-2005-870005