1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine

Base Information

Chemical Name:1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine
CAS No.:348086-41-9
Molecular Formula:C₁₅H₁₃N₇O₄
Molecular Weight:355.313
Hs Code.:

Synonyms:1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine

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Chemical Property of 1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine

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Technology Process of 1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine

There total 1 articles about 1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 39209-25-1
N-p-nitrophenylethanehydrazonoyl chloride

: 85-18-7
1,3-dimethyl-8-chloroxanthine

: 348086-41-9
1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine

Guidance literature:: With triethylamine; In 1,4-dioxane; Heating;
DOI:10.1021/jo001626a

Reference yield: 95.0%

: 348086-41-9
1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine

: 855007-28-2
1-(4-amino-phenyl)-3,5,7-trimethyl-1H,7H-1,2,3a,5,7,8-hexaaza-cyclopenta[a]indene-4,6-dione

Guidance literature:: With hydrazine hydrate; palladium on activated charcoal; In 1,4-dioxane; for 0.333333h; Heating;
DOI:10.1016/j.farmac.2005.01.008

Reference yield:

: 348086-41-9
1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine

: thiophene-2-carboxylic acid [4-(3,5,7-trimethyl-4,6-dioxo-4,5,6,7-tetrahydro-1,2,3a,5,7,8-hexaaza-cyclopenta[a]inden-1-yl)-phenyl]-amide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / hydrazine hydrate / Pd/C / dioxane / 0.33 h / Heating

2: 65 percent / Et₃N / dioxane / 6 h / 20 °C

With hydrazine hydrate; triethylamine; palladium on activated charcoal; In 1,4-dioxane;
DOI:10.1016/j.farmac.2005.01.008