7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine

Base Information

Chemical Name:7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine
CAS No.:1261174-80-4
Molecular Formula:C₁₅H₁₄ClFN₄
Molecular Weight:313.683
Hs Code.:

Synonyms:7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine

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Technology Process of 7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine

There total 2 articles about 7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 446-24-2
2-fluorobezohydrazide

: 1261174-79-1
3,6-dichloro-4-(1,1-dimethylethyl-d9)-pyridazine

: 1261174-80-4
7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine

Guidance literature:: With triethylamine hydrochloride; In xylene; Heating; Reflux;

Reference yield:

: 394-35-4
methyl 2-fluorobenzoate

: 1261174-80-4
7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / Heating; Reflux

2: triethylamine hydrochloride / xylene / Heating; Reflux

With triethylamine hydrochloride; hydrazine hydrate; In ethanol; xylene;

Reference yield: 77.0%

: 1213670-32-6
(1-(methyl-d3)-1H-1,2,4-triazol-5-yl)methanol

: 1261174-80-4
7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine

: 1261174-56-4
3-(2-fluorophenyI)-7-(d9-tert-butyl)-6-((1-d3-methyl-1H-1,2,4-triazol-5-yl)methoxy)-[1,2,4]triazolo[4,3-b]pyridazine

Guidance literature:: (1-(methyl-d3)-1H-1,2,4-triazol-5-yl)methanol; With sodium hydride; In 1-methyl-pyrrolidin-2-one; mineral oil; for 0.25h;

7-(tert-butyl-d9)-6-chloro-3-(2-fluorophenyl)-[1,2,4]triazolo[4,3-b]pyridazine; In 1-methyl-pyrrolidin-2-one; mineral oil; at 20 ℃; for 3h;