2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol

Base Information

Chemical Name:2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol
CAS No.:1333854-02-6
Molecular Formula:C₂₀H₂₄O₇
Molecular Weight:376.406
Hs Code.:

Synonyms:2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol

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Chemical Property of 2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol

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Technology Process of 2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol

There total 3 articles about 2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1333853-96-5
2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol 1,3-diacetate

: 1333854-02-6
2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol

Guidance literature:: 2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol 1,3-diacetate; With sodium methylate; In methanol; at 0 ℃; for 0.5h; Inert atmosphere;

In methanol; pH=7; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.05.021

Reference yield:

: 1333853-90-9
2-(1-bromo-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol 1,3-diacetate

: 1333854-02-6
2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane; water / 24 h / 85 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3.1: sodium methylate / methanol / 0.5 h / 0 °C / Inert atmosphere

3.2: Amberlite IR-120 / pH 7 / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutyl ammonium fluoride; sodium methylate; potassium carbonate; In methanol; 1,2-dimethoxyethane; dichloromethane; water;
DOI:10.1016/j.ejmech.2011.05.021

Reference yield:

: 1333853-93-2
2-(1-(3-tert-butyldimethylsilyloxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol 1,3-diacetate

: 1333854-02-6
2-(1-(3-hydroxy-4-methoxyphenyl)-1-(3,4,5-trimethoxyphenyl)methylene)propan-1,3-diol

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutyl ammonium fluoride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: sodium methylate / methanol / 0.5 h / 0 °C / Inert atmosphere

2.2: Amberlite IR-120 / pH 7 / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium methylate; In methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.05.021