Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

Base Information

Chemical Name:Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol
CAS No.:160654-40-0
Molecular Formula:C₂₀H₁₉N₅O₆S
Molecular Weight:457.467
Hs Code.:

Synonyms:Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

Suppliers and Price of Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

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Technology Process of Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

There total 4 articles about Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 108-24-7
acetic anhydride

: 160654-34-2
(Z)-5-Amino-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

: 160654-40-0
Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

Guidance literature:: for 0.0833333h; Heating;

Reference yield:

: 3431-62-7,20747-39-1
3-nitrobenzaldoxime

: 160654-40-0
Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

Guidance literature:: Multi-step reaction with 4 steps

1: N-chlorosuccinimide / dimethylformamide / 55 - 57 °C

2: 48 percent / Et₃N / dioxane / 3 h / Ambient temperature

3: 72 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

4: 86 percent / 0.08 h / Heating

With N-chloro-succinimide; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 33512-94-6
m-nitrobenzhydroxamoyl chloride

: 160654-40-0
Z-5-Acetamido-3-methyl-1-<(3-nitrophenyl)(p-tosyloximino)methyl>-1H-pyrazol

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / Et₃N / dioxane / 3 h / Ambient temperature

2: 72 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

3: 86 percent / 0.08 h / Heating

With triethylamine; In 1,4-dioxane; acetonitrile;