1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate

Base Information

Chemical Name:1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate
CAS No.:1382764-33-1
Molecular Formula:C₂₄H₂₆N₂O₂S₂
Molecular Weight:438.615
Hs Code.:

Synonyms:1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate

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Chemical Property of 1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate

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Technology Process of 1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate

There total 3 articles about 1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1382764-29-5
1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium triflate

: 1382764-33-1
1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate

Guidance literature:: 1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium triflate; With sodium hexamethyldisilazane; In toluene; at 25 ℃; Inert atmosphere;

With carbon disulfide; In toluene; at 25 ℃; Inert atmosphere;
DOI:10.1021/om300401t

Reference yield:

: 75105-48-5
N,N'-dimesitylformamidine

: 1382764-33-1
1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 3 h / 25 °C / Inert atmosphere

2.1: dichloromethane / 12 h / 25 °C / Inert atmosphere

3.1: sodium hexamethyldisilazane / toluene / 25 °C / Inert atmosphere

3.2: 25 °C / Inert atmosphere

With sodium hexamethyldisilazane; dicyclohexyl-carbodiimide; In dichloromethane; toluene;
DOI:10.1021/om300401t

Reference yield:

: 1382764-27-3
1,3-dimesityl-4-oxo-3,4-dihydropyrimidin-1-ium-6-olate

: 1382764-33-1
1,3-dimesityl-6-methoxy-4-oxo-3,4-dihydropyrimidin-1-ium-2-carbodithioate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 12 h / 25 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / toluene / 25 °C / Inert atmosphere

2.2: 25 °C / Inert atmosphere

With sodium hexamethyldisilazane; In dichloromethane; toluene;
DOI:10.1021/om300401t