((CH(CH₃)2)2C₆H₃N)2CCH₂CHCCH₃BBr

Base Information

• Chemical Name: ((CH(CH₃)2)2C₆H₃N)2CCH₂CHCCH₃BBr
• CAS No.: 1287239-89-7
• Molecular Formula: C₂₉H₄₀BBrN₂
• Molecular Weight: 507.365

Synonyms:((CH(CH₃)2)2C₆H₃N)2CCH₂CHCCH₃BBr

Chemical Property of ((CH(CH₃)2)2C₆H₃N)2CCH₂CHCCH₃BBr

Chemical Property:

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Technology Process of ((CH(CH₃)2)2C₆H₃N)2CCH₂CHCCH₃BBr

There total 4 articles about ((CH(CH₃)2)2C₆H₃N)2CCH₂CHCCH₃BBr which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine (210832-39-6) → ((CH(CH3)2)2C6H3N)2CCH2CHCCH3BBr (1287239-89-7)

Guidance literature:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine; With n-butyllithium; In diethyl ether; hexane; at -78 - 20 ℃; Inert atmosphere;

With Et₃N*BBr₃; In diethyl ether; hexane; at 20 ℃; Inert atmosphere;

DOI:10.1002/anie.201007417

Reference yield: 28.0%

((CH(CH3)2)2C6H3NCCH3)2CHBBr(1+)*BBr4(1-)=((CH(CH3)2)2C6H3NCCH3)2CHBBr(BBr4) → ((CH(CH3)2)2C6H3N)2CCH2CHCCH3BBr (1287239-89-7)

Guidance literature:

With lithium dihydronaphthylide radical; In tetrahydrofuran; at -78 ℃; for 2h; Inert atmosphere;

DOI:10.1039/c1cc11789k

Reference yield:

2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-2-pentene → ((CH(CH3)2)2C6H3N)2CCH2CHCCH3BBr (1287239-89-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: n-butyllithium / hexane; toluene / 5 h / -78 - 20 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: lithium dihydronaphthylide radical / tetrahydrofuran / 2 h / -78 °C / Inert atmosphere

With n-butyllithium; lithium dihydronaphthylide radical; In tetrahydrofuran; hexane; toluene;

DOI:10.1039/c1cc11789k

upstream raw materials:

N,N′-bis(2,6-diisopropylphenyl)pentane-2,4-diimine

Li(2,6-iPr₂C₆H₃)NC(Me)CHC(Me)N(2,6-iPr₂C₆H₃)

Downstream raw materials:

borinic acid

B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2^(1-)*N₂C₃H(CH₃)4⁽¹⁺⁾=[B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2][N₂C₃H(CH₃)4]

B(O)N₂C₃H(CH₃)(CH₂)(C₆H₃(CH(CH₃)2)2)2^(1-)*N₂C₃H(CH₃)2(CH(CH₃)2)2⁽¹⁺⁾=BO(C₄₀H₆₁N₄)

(BF₂)N₂C₃H(CH₃)2(C₆H₃(CH(CH₃)2)2)2

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