N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide

Base Information

Chemical Name:N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide
CAS No.:175469-69-9
Molecular Formula:C₂₈H₄₇NO₁₁
Molecular Weight:573.681
Hs Code.:

N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide

Synonyms:N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide

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Chemical Property of N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide

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Technology Process of N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide

There total 10 articles about N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 175469-68-8
Benzoic acid 2-[(3aR,4S,6S,7S,7aR)-6-((4aR,6R,7R,8R,8aS)-7-acetylamino-6-cyclohexyloxy-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-8-yloxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yloxy]-ethyl ester

: 175469-69-9
N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide

Guidance literature:: With potassium tert-butylate; In methanol; for 16h;

Reference yield:

: 21559-72-8
cyclohexyl 2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 175469-69-9
N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: p-TsOH / acetone / 4 h / 40 °C

2: 0.4 nm molecular sieves, CuBr₂, Bu₄NBr / 1,2-dichloro-ethane; dimethylformamide / 16 h

3: 91 percent / t-BuOK / methanol / 16 h

With 4 A molecular sieve; potassium tert-butylate; tetrabutylammomium bromide; toluene-4-sulfonic acid; copper(ll) bromide; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;

Reference yield:

: 21588-60-3
cyclohexyl 3,4,6-tri-O-acetyl-2-(acetylamino)-2-deoxy-β-D-glucopyranoside

: 175469-69-9
N-{(4aR,6R,7R,8R,8aS)-6-Cyclohexyloxy-8-[(3aR,4S,6S,7S,7aR)-7-(2-hydroxy-ethoxy)-2,2,4-trimethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-6-yloxy]-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxin-7-yl}-acetamide

Guidance literature:: Multi-step reaction with 4 steps

1: NaOMe / methanol / 2 h

2: p-TsOH / acetone / 4 h / 40 °C

3: 0.4 nm molecular sieves, CuBr₂, Bu₄NBr / 1,2-dichloro-ethane; dimethylformamide / 16 h

4: 91 percent / t-BuOK / methanol / 16 h

With 4 A molecular sieve; potassium tert-butylate; tetrabutylammomium bromide; sodium methylate; toluene-4-sulfonic acid; copper(ll) bromide; In methanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;