3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

Base Information

Chemical Name:3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose
CAS No.:1012796-20-1
Molecular Formula:C₂₅H₃₅N₃O₁₀
Molecular Weight:537.567
Hs Code.:

Synonyms:3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

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Chemical Property of 3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

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Technology Process of 3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

There total 1 articles about 3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1738-86-9
Z-Gly-ONp

: 449205-67-8
(3R)-1,2:5,6-di-O-isopropylidene-spiro[3-deoxy-α-D-ribohexofuranose-3,5'-piperazine]-2'-one

: 1012796-20-1
3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

Guidance literature:: (3R)-1,2:5,6-di-O-isopropylidene-spiro[3-deoxy-α-D-ribohexofuranose-3,5'-piperazine]-2'-one; With sodium hydroxide; water; In 1,4-dioxane; at 100 ℃;

Z-Gly-ONp; In 1,4-dioxane; water; at 20 ℃; for 1h; Further stages.;
DOI:10.1016/j.tetasy.2007.11.038

Reference yield: 67.0%

: 1012796-20-1
3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 10065-72-2
L-Alanine methyl ester

: 1012796-24-5
3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-deoxy-1,2:5,6-di-O-isopropylidene-3-[({[(S)-1-(methoxycarbonyl)ethyl]amino}carbonyl)methylamino]-α-D-allofuranose

Guidance literature:: With 1-hydroxy-pyrrolidine-2,5-dione; triethylamine; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile; at -10 - 20 ℃; for 24h;
DOI:10.1016/j.tetasy.2007.11.038

Reference yield:

: 1012796-20-1
3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-β-D-allopyranose

: 3-C-[(N-benzyloxycarbonylglycyl)aminomethyl]-3-[(carboxymethyl)amino]-3-deoxy-α-D-allopyranose

Guidance literature:: With water; trifluoroacetic acid; at 20 ℃; Title compound not separated from byproducts.;
DOI:10.1016/j.tetasy.2007.11.038