C₁₆H₁₃Br

Base Information

• Chemical Name: C₁₆H₁₃Br
• CAS No.: 1416331-74-2
• Molecular Formula: C₁₆H₁₃Br
• Molecular Weight: 285.183
• Mol file: 1416331-74-2.mol

Synonyms:C₁₆H₁₃Br

Chemical Property of C₁₆H₁₃Br

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₆H₁₃Br

There total 1 articles about C₁₆H₁₃Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4-bromophenyl)(phenyl)methanone (90-90-4) + 3-bromopropyltriphenylphosphonium bromide (3607-17-8) → C16H13Br (1416331-74-2)

Guidance literature:

3-bromopropyltriphenylphosphonium bromide; With sodium hydride; In tetrahydrofuran; at 70 ℃; Inert atmosphere;

(4-bromophenyl)(phenyl)methanone; In tetrahydrofuran; at 70 ℃;

DOI:10.1021/acs.orglett.7b02989

Reference yield: 83.0%

C16H13Br (1416331-74-2) + 1-(p-toluenesulfonylamino)-pyridinium tetrafluoroborate → N-tosyl-2-(4-bromophenyl)-2-phenylcyclobutanimine

Guidance literature:

With tris[2-phenylpyridinato-C₂,N]iridium(III); In acetonitrile; at 20 ℃; for 36h; Irradiation; Inert atmosphere;

DOI:10.1021/acs.orglett.7b02989

Reference yield: 58.0%

C16H13Br (1416331-74-2) → 3-[(4-bromophenyl)(phenyl)methylene]-1,2-dithiolane

Guidance literature:

With sulfur; In 1,2-dichloro-ethane; at 80 ℃; for 27h; Inert atmosphere; Schlenk technique;

DOI:10.1021/ol3031846

upstream raw materials:

(4-bromophenyl)(phenyl)methanone

3-bromopropyltriphenylphosphonium bromide