(3S,4S,S_S)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene

Base Information

• Chemical Name: (3S,4S,S_S)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene
• CAS No.: 223125-12-0
• Molecular Formula: C₁₉H₃₀O₄S
• Molecular Weight: 354.511

Synonyms:(3S,4S,S_S)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene

Chemical Property of (3S,4S,S_S)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene

Chemical Property:

Purity/Quality:

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Technology Process of (3S,4S,S_S)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene

There total 3 articles about (3S,4S,S_S)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S-exo)-2-bornyl 2-cyanoethylsulfoxide → (3S,4S,SS)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene (223125-12-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 48 percent / xylene / 0.33 h / Heating

2: CH₂Cl₂ / 480 h / Ambient temperature

In dichloromethane; xylene;

DOI:10.1021/jo981262a

Reference yield:

acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) + (SS,E)-3-<(1S,exo)-2-bornylsulfinyl>-1-methoxybuta-1,3-diene (223125-01-7) → (3R,4R,SS)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene + (3S,4S,SS)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene (223125-12-0)

Guidance literature:

With lithium perchlorate; In dichloromethane; for 5h; Yield given; Yields of byproduct given; Ambient temperature;

DOI:10.1021/jo981262a

Reference yield:

acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) + (SS,E)-3-<(1S,exo)-2-bornylsulfinyl>-1-methoxybuta-1,3-diene (223125-01-7) → (3R,4R,SS)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene + (1S,2R)-2-Methoxy-4-((S)-(1S,2S,4S)-1,7,7-trimethyl-bicyclo[2.2.1]heptane-2-sulfinyl)-cyclohex-3-enecarboxylic acid methyl ester + (1R,2S)-2-Methoxy-4-((S)-(1S,2S,4S)-1,7,7-trimethyl-bicyclo[2.2.1]heptane-2-sulfinyl)-cyclohex-3-enecarboxylic acid methyl ester + (3S,4S,SS)-1-<(1S-exo)-2-bornylsulfinyl>-3-methoxy-4-methoxycarbonylcyclohexene (223125-12-0)

Guidance literature:

In dichloromethane; for 480h; Yield given; Yields of byproduct given; Ambient temperature;

DOI:10.1021/jo981262a

upstream raw materials:

acrylic acid methyl ester

(S_S,E)-3-<(1S,exo)-2-bornylsulfinyl>-1-methoxybuta-1,3-diene

Downstream raw materials:

(3S,4S)-1-<(1S-exo)-2-bornylsulfonyl>-3-methoxy-4-methoxycarbonylcyclohexene

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