ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate

Base Information

Chemical Name:ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate
CAS No.:1207268-93-6
Molecular Formula:C₃₀H₃₀F₃N₃O₄S
Molecular Weight:585.647
Hs Code.:

Synonyms:ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate

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Chemical Property of ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate

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Technology Process of ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate

There total 10 articles about ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 600-00-0
ethyl 2-bromoisobutyrate

: 1207269-28-0
C₂₄H₂₀F₃N₃O₂S

: 1207268-93-6
ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate

Guidance literature:: With potassium carbonate; In acetonitrile; for 36h; Reflux;

Reference yield:

: 103-82-2
phenylacetic acid

: 1207268-93-6
ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate

Guidance literature:: Multi-step reaction with 7 steps

1: sulfuric acid / 2 h / Reflux

2: water / 3 h / Reflux

3: trichlorophosphate / toluene / 5 h / 80 - 90 °C

4: dmap / tetrahydrofuran / 12 h / 20 °C

5: dibenzoyl peroxide; N-Bromosuccinimide / chloroform / 12 h / Reflux

6: potassium carbonate / acetonitrile / 6 h / 20 °C

7: potassium carbonate / acetonitrile / 36 h / Reflux

With dmap; N-Bromosuccinimide; sulfuric acid; potassium carbonate; trichlorophosphate; dibenzoyl peroxide; In tetrahydrofuran; chloroform; water; toluene; acetonitrile;

Reference yield:

: 95-48-7,77504-84-8
ortho-cresol

: 1207268-93-6
ethyl 2,2-dimethyl-2-(3-methyl-4-(1-(2-(4-methyl-5-oxo-1-(4-trifluoromethylphenyl)-4,5-dihydrogen-1H-1,2,4.triazolyl))-benzylthio)-phenoxy)-acetate

Guidance literature:: Multi-step reaction with 4 steps

1: bromine; sodium bromide / methanol / 5 h / 0 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 - 20 °C

3: potassium carbonate / acetonitrile / 6 h / 20 °C

4: potassium carbonate / acetonitrile / 36 h / Reflux

With lithium aluminium tetrahydride; bromine; potassium carbonate; sodium bromide; In tetrahydrofuran; methanol; acetonitrile;