N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide

Base Information

Chemical Name:N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide
CAS No.:160422-47-9
Molecular Formula:C₂₆H₃₆INO₄SSi
Molecular Weight:613.632
Hs Code.:

Synonyms:N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide

Suppliers and Price of N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide

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Chemical Property of N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide

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Technology Process of N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide

There total 4 articles about N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 160422-47-9
N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / Ambient temperature

2: 92 percent / I₂, HIO₃ / methanol; H₂O / 48 h / Heating

3: 1.) NaH / 1.) DMF, 0 deg C, 2.) DMF, 50 deg C

With dmap; iodine; iodic acid; sodium hydride; triethylamine; In methanol; dichloromethane; water;

Reference yield:

: 120-20-7
2-(3,4-dimethoxyphenyl)-ethylamine

: 160422-47-9
N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / Ambient temperature

2: 92 percent / I₂, HIO₃ / methanol; H₂O / 48 h / Heating

3: 1.) NaH / 1.) DMF, 0 deg C, 2.) DMF, 50 deg C

With dmap; iodine; iodic acid; sodium hydride; triethylamine; In methanol; dichloromethane; water;

Reference yield:

: 160422-44-6
N-<2-(3,4-dimethoxyphenyl)ethyl>mesitylenesulfonamide

: 160422-47-9
N-<2-(2-iodo-4,5-dimethoxyphenyl)ethyl>-N-<4-(trimethylsilyl)but-2-ynyl>mesitylenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / I₂, HIO₃ / methanol; H₂O / 48 h / Heating

2: 1.) NaH / 1.) DMF, 0 deg C, 2.) DMF, 50 deg C

With iodine; iodic acid; sodium hydride; In methanol; water;