2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate

Base Information

Chemical Name:2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate
CAS No.:119117-31-6
Molecular Formula:C₁₉H₁₈BrFO₄
Molecular Weight:409.252
Hs Code.:

Synonyms:2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate

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Chemical Property of 2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate

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Technology Process of 2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate

There total 5 articles about 2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 119117-30-5
2-benzoyloxymethyl-2-fluoro-4-hydroxybutyl benzoate

: 119117-31-6
2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In N,N-dimethyl-formamide; at 25 ℃; for 2.5h;

Reference yield:

: 119117-21-4
4-benzyloxy-2-hydroxymethylbutane-1,2-diol

: 119117-31-6
2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / pyridine / 2 h / 25 °C

2: 89 percent / calcium carbonate, diethylaminosulphur trifluoride / 1,2-dichloro-ethane / 2 h / 25 °C

3: 90 percent / H₂ / 10percent palladium-on-charcoal / ethanol; H₂O; acetic acid / 48 h

4: 50 percent / carbon tetrabromide, triphenylphosphine / dimethylformamide / 2.5 h / 25 °C

With pyridine; carbon tetrabromide; diethylamino-sulfur trifluoride; hydrogen; triphenylphosphine; calcium carbonate; palladium on activated charcoal; In ethanol; water; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 119117-20-3
diethyl acetoxy(2-benzyloxyethyl)malonate

: 119117-31-6
2-benzoyloxymethyl-4-bromo-2-fluorobutyl benzoate

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / lithium aluminium hydride / tetrahydrofuran / 2 h / 25 °C

2: 67 percent / pyridine / 2 h / 25 °C

3: 89 percent / calcium carbonate, diethylaminosulphur trifluoride / 1,2-dichloro-ethane / 2 h / 25 °C

4: 90 percent / H₂ / 10percent palladium-on-charcoal / ethanol; H₂O; acetic acid / 48 h

5: 50 percent / carbon tetrabromide, triphenylphosphine / dimethylformamide / 2.5 h / 25 °C

With pyridine; lithium aluminium tetrahydride; carbon tetrabromide; diethylamino-sulfur trifluoride; hydrogen; triphenylphosphine; calcium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; water; acetic acid; 1,2-dichloro-ethane; N,N-dimethyl-formamide;