2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one

Base Information

Chemical Name:2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one
CAS No.:101905-30-0
Molecular Formula:C₂₅H₂₅ClO₅
Molecular Weight:440.924
Hs Code.:

Synonyms:2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one

Suppliers and Price of 2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one

There total 2 articles about 2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 101923-12-0
1-<6'-benzyloxy-3',4'-dimethoxy-2'-(prop-1-enyl)phenyl>-4-(2-methyl-1,3-dioxolan-2-yl)-2-methylenebutane-1,3-dione

: 101905-29-7
1-benzyloxy-5a,b-dihydro-3-methoxy-5,9-dimethylbenzofuro<3,4-gh>-<1>benzopyran-7(5H)-one

: 101905-30-0
2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one

Guidance literature:: With hydrogenchloride; In acetic acid;
DOI:10.1039/c39850001483

Reference yield: 73.0%

: 95730-77-1
1-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-4-(2-methyl-1,3-dioxolan-2-yl)-2-(methylsulphinylmethyl)butane-1,3-dione

: 101905-29-7
1-benzyloxy-5a,b-dihydro-3-methoxy-5,9-dimethylbenzofuro<3,4-gh>-<1>benzopyran-7(5H)-one

: 101905-30-0
2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one

Guidance literature:: With hydrogenchloride; In acetic acid; for 24h; Ambient temperature;
DOI:10.1039/P19870000395

Reference yield:

: 101905-30-0
2-<6-benzyloxy-3,4-dimethoxy-2-(prop-1-enyl)phenyl>-3-chloromethyl-6-methyl-4H-pyran-4-one

: 478-60-4
Citromycetin

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent

2: 69 percent / NaHCO₃ / methanol; H₂O

3: O₃, Oil Violet

4: sodium chlorite, sulphamic acid

5: 69 percent / AlCl₃, Me₂S / CH₂Cl₂

With sodium chlorite; aluminium trichloride; dimethylsulfide; oil violet; aminosulfonic acid; sodium hydrogencarbonate; ozone; In methanol; dichloromethane; water;
DOI:10.1039/c39850001483