C₆₃H₈₈OSi₂

Base Information

Chemical Name:C₆₃H₈₈OSi₂
CAS No.:1313995-13-9
Molecular Formula:C₆₃H₈₈OSi₂
Molecular Weight:917.562
Hs Code.:

C<sub>63</sub>H<sub>88</sub>OSi<sub>2</sub>

Synonyms:C₆₃H₈₈OSi₂

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Chemical Property of C₆₃H₈₈OSi₂

Chemical Property:

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Technology Process of C₆₃H₈₈OSi₂

There total 9 articles about C₆₃H₈₈OSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1313995-12-8
C₄₁H₄₆I₂O

: 89343-06-6
tris-iso-propylsilyl acetylene

: 1313995-13-9
C₆₃H₈₈OSi₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; Inert atmosphere;
DOI:10.1039/c1ob05441d

Reference yield:

: 1313995-16-2
2,6-diiodo-4-octylaniline

: 1313995-13-9
C₆₃H₈₈OSi₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid; sodium nitrite / -5 °C

1.2: Reflux

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sulfuric acid; N-ethyl-N,N-diisopropylamine; sodium nitrite; In tetrahydrofuran; 2.1: Castro-Stephen-Sonogashira coupling / 3.1: Castro-Stephen-Sonogashira coupling;
DOI:10.1039/c1ob05441d

Reference yield:

: 1313995-11-7
C₁₉H₂₄OSi₂

: 1313995-13-9
C₆₃H₈₈OSi₂

Guidance literature:: Multi-step reaction with 3 steps

1: water; potassium hydroxide / tetrahydrofuran; methanol / 0.25 h

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; water; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In tetrahydrofuran; methanol; 2: Castro-Stephen-Sonogashira coupling / 3: Castro-Stephen-Sonogashira coupling;
DOI:10.1039/c1ob05441d