exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester

Base Information

Chemical Name:exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester
CAS No.:681424-95-3
Molecular Formula:C₂₂H₂₂F₂N₂O₄
Molecular Weight:416.424
Hs Code.:

Synonyms:exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester

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Chemical Property of exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester

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Technology Process of exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester

There total 1 articles about exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 681424-96-4
C₁₄H₁₆F₂N₂O₂

: 501-53-1,94274-21-2
benzyl chloroformate

: 681424-95-3
exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester

Guidance literature:: With pyridine; at 0 - 20 ℃; for 1h;

Reference yield:

: 681424-95-3
exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester

: 681424-98-6
exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid

Guidance literature:: exo-(1R,5S)-3-(4-benzyloxycarbonylamino-2,6-difluoro-phenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid ethyl ester; With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran; at 20 ℃; for 72h;

With hydrogenchloride; In water;