carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-1-{3-[tert-butyl(dimethyl)silyl]oxy}propyl-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

Base Information

• Chemical Name: carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-1-{3-[tert-butyl(dimethyl)silyl]oxy}propyl-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester
• CAS No.: 1196064-24-0
• Molecular Formula: C₄₉H₇₉NO₇Si₃
• Molecular Weight: 878.425

Synonyms:carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-1-{3-[tert-butyl(dimethyl)silyl]oxy}propyl-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

Chemical Property of carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-1-{3-[tert-butyl(dimethyl)silyl]oxy}propyl-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

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Technology Process of carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-1-{3-[tert-butyl(dimethyl)silyl]oxy}propyl-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

There total 1 articles about carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-1-{3-[tert-butyl(dimethyl)silyl]oxy}propyl-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C51H78Cl3NO8Si3 → carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-1-{3-[tert-butyl(dimethyl)silyl]oxy}propyl-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester (1196064-24-0)

Guidance literature:

With methanol; potassium carbonate; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1055/s-0029-1216921

Reference yield: 75.0%

carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-1-{3-[tert-butyl(dimethyl)silyl]oxy}propyl-2-{[tert-butyl(diphenyl)silyl]oxy}-9-[(4-methoxybenzyl)oxy]non-3-enyl ester (1196064-24-0) → carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-(3-hydropropyl)-9-[(4-methoxybenzyl)oxy]non-3-enyl ester (1196064-25-1)

Guidance literature:

With water; acetic acid; In tetrahydrofuran; at 20 ℃; for 12h;

DOI:10.1055/s-0029-1216921

Downstream raw materials:

carbamic acid (1S,2S,3E,5S)-5-{[tert-butyl(dimethyl)silyl]oxy}-2-{[tert-butyl(diphenyl)silyl]oxy}-1-(3-hydropropyl)-9-[(4-methoxybenzyl)oxy]non-3-enyl ester

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