C₃₂H₅₁SiNO₈

Base Information

Chemical Name:C₃₂H₅₁SiNO₈
CAS No.:937164-18-6
Molecular Formula:C₃₂H₅₁NO₈Si
Molecular Weight:605.844
Hs Code.:

C<sub>32</sub>H<sub>51</sub>SiNO<sub>8</sub>

Synonyms:C₃₂H₅₁SiNO₈

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Chemical Property of C₃₂H₅₁SiNO₈

Chemical Property:

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Technology Process of C₃₂H₅₁SiNO₈

There total 11 articles about C₃₂H₅₁SiNO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 937163-86-5
C₃₅H₅₉Si₂NO₈

: 937164-18-6
C₃₂H₅₁SiNO₈

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃;
DOI:10.1021/ol070435s

Reference yield:

: 937164-09-5
C₂₂H₃₄SiO₄

: 937164-18-6
C₃₂H₅₁SiNO₈

Guidance literature:: Multi-step reaction with 9 steps

1: 87 percent / P₂O₅ / 0.5 h / 20 °C

2: 73 percent / DIBAL-H / CH₂Cl₂ / 1 h / -78 °C

3: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

4: 82 percent / NIS / CH₂Cl₂ / 20 °C

5: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

6: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

7: ceric ammonium nitrate / acetonitrile; H₂O / 1 h / 20 °C

8: 0.29 g / K₂CO₃ / acetone; H₂O / 0.17 h / 20 °C

9: 95 percent / K₂CO₃ / methanol / 20 °C

With N-iodo-succinimide; ammonium cerium(IV) nitrate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; phosphorus pentoxide; diisobutylaluminium hydride; potassium carbonate; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/ol070435s

Reference yield:

: 937163-73-0
C₁₇H₃₄SiO₄

: 937164-18-6
C₃₂H₅₁SiNO₈

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / triethylamine / (methoxymethylcarbene)pentacarbonyl tungsten / tetrahydrofuran / 24 h / 60 °C

2: 82 percent / NIS / CH₂Cl₂ / 20 °C

3: 88 percent / HSnBu₃; AIBN / toluene / 5 h / 80 °C

4: 90 percent / tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

5: ceric ammonium nitrate / acetonitrile; H₂O / 1 h / 20 °C

6: 0.29 g / K₂CO₃ / acetone; H₂O / 0.17 h / 20 °C

7: 95 percent / K₂CO₃ / methanol / 20 °C

With N-iodo-succinimide; ammonium cerium(IV) nitrate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; potassium carbonate; triethylamine; (methoxymethylcarbene)pentacarbonyl tungsten; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/ol070435s