C₁₆H₂₀N₃O₅P

Base Information

• Chemical Name: C₁₆H₂₀N₃O₅P
• CAS No.: 1333165-97-1
• Molecular Formula: C₁₆H₂₀N₃O₅P
• Molecular Weight: 365.326
• Mol file: 1333165-97-1.mol

Synonyms:C₁₆H₂₀N₃O₅P

Chemical Property of C₁₆H₂₀N₃O₅P

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₁₆H₂₀N₃O₅P

There total 1 articles about C₁₆H₂₀N₃O₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + 1-(diethoxyphosphonyl)buta-1,3-diene (7158-35-2) → C16H20N3O5P (1333165-97-1)

Guidance literature:

In 1,2-dichloro-ethane; at 120 ℃; for 0.5h; Sealed tube; Microwave irradiation;

DOI:10.1016/j.tetlet.2011.07.116

Reference yield: 99.0%

C16H20N3O5P (1333165-97-1) → C12H12N3O5P

Guidance literature:

C₁₆H₂₀N₃O₅P; With trimethylsilyl bromide; In dichloromethane; at 20 ℃; for 96h; Inert atmosphere;

With methanol; In dichloromethane; at 20 ℃; for 1h;

DOI:10.3987/COM-12-12653

Reference yield: 98.0%

C16H20N3O5P (1333165-97-1) → C16H22N3O5P

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 18h; under 760.051 Torr;

DOI:10.3987/COM-12-12653

upstream raw materials:

4-Phenyl-1,2,4-triazolidine-3,5-dione

1-(diethoxyphosphonyl)buta-1,3-diene