2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate

Base Information

Chemical Name:2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate
CAS No.:1266398-35-9
Molecular Formula:C₂₇H₁₆F₉O₄PS
Molecular Weight:638.447
Hs Code.:

Synonyms:2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate

Chemical Property:

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Technology Process of 2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate

There total 3 articles about 2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1266398-34-8
2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-ol

: 1266398-35-9
2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate

Guidance literature:: With pyridine; dmap; In dichloromethane; at 0 ℃; Reflux;
DOI:10.1007/s11426-010-4172-z

Reference yield:

: C₂₆H₁₇F₆OP

: 1266398-35-9
2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / dichloromethane; water / 0 - 20 °C

2: pyridine; dmap / dichloromethane / 0 °C / Reflux

With pyridine; dmap; dihydrogen peroxide; In dichloromethane; water;
DOI:10.1007/s11426-010-4172-z

Reference yield:

: 22749-43-5
p-chlorodibenzo[c.e][1,2]oxaphosphorine

: 1266398-35-9
2'-(bis(4-(trifluoromethyl)phenyl)phosphoryl)biphenyl-2-yltrifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: iodine; magnesium / 2 h / 50 °C / Inert atmosphere; Reflux

1.2: 25 °C / Inert atmosphere; Reflux

1.3: 0 °C / Inert atmosphere

2.1: dihydrogen peroxide / dichloromethane; water / 0 - 20 °C

3.1: pyridine; dmap / dichloromethane / 0 °C / Reflux

With pyridine; dmap; dihydrogen peroxide; iodine; magnesium; In dichloromethane; water;
DOI:10.1007/s11426-010-4172-z