(10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide

Base Information

Chemical Name:(10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide
CAS No.:98050-16-9
Molecular Formula:Br*C₃₀H₃₄O₂P
Molecular Weight:537.477
Hs Code.:

Synonyms:(10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide

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Chemical Property of (10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide

Chemical Property:

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Technology Process of (10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide

There total 18 articles about (10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 88158-73-0
11-bromo-undeca-5,8-cis,cis-dienoic acid methyl ester

: 603-35-0
triphenylphosphine

: 98050-16-9
(10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide

Guidance literature:: DOI:10.1021/jo00033a006

Reference yield:

: 96188-15-7
cis,cis-11-oxo-undeca-5,8-dienoic acid methyl ester

: 98050-16-9
(10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / sodium borohydride / methanol / 0.17 h / 0 °C

2: 86 percent / triphenylphosphine; carbon tetrabromide / CH₂Cl₂ / 2 h / 20 °C

3: 100 percent / 24 h / Heating

With sodium tetrahydroborate; carbon tetrabromide; triphenylphosphine; In methanol; dichloromethane;
DOI:10.1021/ja026880u

Reference yield:

: 125112-18-7
11-hydroxy-undeca-5,8-cis,cis-dienoic acid methyl ester

: 98050-16-9
(10-methoxycarbonyldeca-3,6-cis,cis-dienyl)-triphenylphosphonium bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / triphenylphosphine; carbon tetrabromide / CH₂Cl₂ / 2 h / 20 °C

2: 100 percent / 24 h / Heating

With carbon tetrabromide; triphenylphosphine; In dichloromethane;
DOI:10.1021/ja026880u