C₃₃H₄₇N₃O₇

Base Information

Chemical Name:C₃₃H₄₇N₃O₇
CAS No.:1079399-12-4
Molecular Formula:C₃₃H₄₇N₃O₇
Molecular Weight:597.752
Hs Code.:

C<sub>33</sub>H<sub>47</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₃₃H₄₇N₃O₇

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Chemical Property of C₃₃H₄₇N₃O₇

Chemical Property:

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Technology Process of C₃₃H₄₇N₃O₇

There total 18 articles about C₃₃H₄₇N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1079399-11-3
C₂₈H₃₉N₃O₅

: 24424-99-5
di-tert-butyl dicarbonate

: 1079399-12-4
C₃₃H₄₇N₃O₇

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 6.5h;

Reference yield:

: 2398-37-0
3-methoxyphenyl bromide

: 1079399-12-4
C₃₃H₄₇N₃O₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: magnesium / iodine / tetrahydrofuran / 4 h / Heating / reflux

2.1: boron tribromide / dichloromethane / 3 h / 0 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 17 h / 20 - 110 °C

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.25 h / -15 °C

4.2: 12.5 h / -15 - 20 °C

5.1: hydrogenchloride / 3 h / 0 - 20 °C

6.1: silver(l) oxide / N,N-dimethyl-formamide / 14 h / 20 °C

7.1: sulfuric acid; water / 1,4-dioxane / 3 h / 20 °C / Heating / reflux

8.1: dipyridinium dichromate / dichloromethane / 10 h / 0 - 20 °C / Molecular sieve

9.1: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 70 °C

10.1: pyridine / 12.67 h / 0 - 20 °C

11.1: potassium superoxide / 18-crown-6 ether / 1,2-dimethoxyethane; dimethyl sulfoxide / 0.5 h / 0 °C

12.1: triphenylphosphine / methanol; water / 16 h / 20 °C

13.1: triethylamine / dichloromethane / 6.5 h / 0 - 20 °C

With pyridine; 2-hydroxypyridin; hydrogenchloride; potassium superoxide; dipyridinium dichromate; di-isopropyl azodicarboxylate; sulfuric acid; water; boron tribromide; potassium carbonate; magnesium; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; silver(l) oxide; 18-crown-6 ether; iodine; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 1079398-41-6
5-[2-(3-allyl-phenoxy)-1-azido-ethyl]-3-methoxy-dihydro-furan-2-one

: 1079399-12-4
C₃₃H₄₇N₃O₇

Guidance literature:: Multi-step reaction with 5 steps

1: 2-hydroxypyridin; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 h / 70 °C

2: pyridine / 12.67 h / 0 - 20 °C

3: potassium superoxide / 18-crown-6 ether / 1,2-dimethoxyethane; dimethyl sulfoxide / 0.5 h / 0 °C

4: triphenylphosphine / methanol; water / 16 h / 20 °C

5: triethylamine / dichloromethane / 6.5 h / 0 - 20 °C

With pyridine; 2-hydroxypyridin; potassium superoxide; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 18-crown-6 ether; In methanol; 1,2-dimethoxyethane; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;