C₁₇H₂₅N

Base Information

Chemical Name:C₁₇H₂₅N
CAS No.:1422558-58-4
Molecular Formula:C₁₇H₂₅N
Molecular Weight:243.392
Hs Code.:

Synonyms:C₁₇H₂₅N

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Chemical Property of C₁₇H₂₅N

Chemical Property:

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Technology Process of C₁₇H₂₅N

There total 4 articles about C₁₇H₂₅N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1422558-36-8
4,4,5,5-tetramethyl-2-(spiro[3.4]nonan-2-ylmethyl)-1,3,2-dioxaborolane

: 622-79-7
benzyl azide

: 1422558-58-4
C₁₇H₂₅N

Guidance literature:: 4,4,5,5-tetramethyl-2-(spiro[3.4]nonan-2-ylmethyl)-1,3,2-dioxaborolane; With boron trichloride; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

benzyl azide; In dichloromethane; at 0 ℃; for 16h;

With sodium hydroxide; In dichloromethane; water;
DOI:10.1021/ja3104582

Reference yield:

: 67838-02-2
methyl 1-allylcyclohexane-1-carboxylate

: 1422558-58-4
C₁₇H₂₅N

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 °C

2.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0.33 h / 0 °C

3.1: copper(l) chloride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium tert-butylate / tetrahydrofuran / 4 h / 30 °C / Inert atmosphere

4.1: boron trichloride / dichloromethane / 4 h / 20 °C / Inert atmosphere

4.2: 16 h / 0 °C

With lithium aluminium tetrahydride; carbon tetrabromide; potassium tert-butylate; boron trichloride; triphenylphosphine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; copper(l) chloride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/ja3104582

Reference yield:

: 67838-03-3
1-(1-(2-propenyl)cyclohexyl)methanol

: 1422558-58-4
C₁₇H₂₅N

Guidance literature:: Multi-step reaction with 3 steps

1.1: carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 0.33 h / 0 °C

2.1: copper(l) chloride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; potassium tert-butylate / tetrahydrofuran / 4 h / 30 °C / Inert atmosphere

3.1: boron trichloride / dichloromethane / 4 h / 20 °C / Inert atmosphere

3.2: 16 h / 0 °C

With carbon tetrabromide; potassium tert-butylate; boron trichloride; triphenylphosphine; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; copper(l) chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja3104582