C₂₈H₂₉N₃O₃

Base Information Edit

Chemical Name:C₂₈H₂₉N₃O₃
CAS No.:1312609-75-8
Molecular Formula:C₂₈H₂₉N₃O₃
Molecular Weight:455.557
Hs Code.:
Mol file:1312609-75-8.mol

C<sub>28</sub>H<sub>29</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₈H₂₉N₃O₃

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Chemical Property of C₂₈H₂₉N₃O₃ Edit

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Technology Process of C₂₈H₂₉N₃O₃

There total 5 articles about C₂₈H₂₉N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1007882-59-8
(S)-2-(4-bromo-1H-imidazol-2-yl)pyrrolidine-1-carboxylic acid tert-butyl ester

: 1312609-74-7
C₂₂H₂₃BO₃

: 1312609-75-8
C₂₈H₂₉N₃O₃

Guidance literature:: With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; water; Inert atmosphere; Reflux;

Reference yield:

: 2298-07-9
4-Bromo-1-naphthylamine

: 1312609-75-8
C₂₈H₂₉N₃O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; tetrahydrofuran / Inert atmosphere; Reflux

3.1: boron tribromide / dichloromethane / 3.5 h / -30 - 20 °C / Inert atmosphere

4.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 4 h / Inert atmosphere; Reflux

5.1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; tetrahydrofuran / Inert atmosphere; Reflux

With hydrogenchloride; potassium acetate; boron tribromide; sodium carbonate; sodium nitrite; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 2.1: Suzuki Coupling / 5.1: Suzuki Coupling;

Reference yield:

: 63279-58-3
1-iodo-4-bromo-naphthalene

: 1312609-75-8
C₂₈H₂₉N₃O₃

Guidance literature:: Multi-step reaction with 4 steps

1: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; tetrahydrofuran / Inert atmosphere; Reflux

2: boron tribromide / dichloromethane / 3.5 h / -30 - 20 °C / Inert atmosphere

3: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 4 h / Inert atmosphere; Reflux

4: sodium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / water; tetrahydrofuran / Inert atmosphere; Reflux

With potassium acetate; boron tribromide; sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; 1: Suzuki Coupling / 4: Suzuki Coupling;