(R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene

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Chemical Name:(R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene
CAS No.:84369-92-6
Molecular Formula:C₁₈H₃₂O₂
Molecular Weight:280.451
Hs Code.:

Synonyms:(R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene

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Chemical Property of (R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene

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Technology Process of (R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene

There total 5 articles about (R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 84393-94-2
(1S,2S)-2-((S)-1-Hydroxymethyl-4-methyl-cyclohex-3-enyl)-2-methyl-cyclopentanol

: 84369-92-6
(R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene

Guidance literature:: Multi-step reaction with 4 steps

1: DBN / dimethylformamide / 0.25 h / 22 °C

2: PPTS / CH₂Cl₂

3: LiAlH₄ / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; 2,6-dichloro-benzonitrile; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00151a034

Reference yield:

: 84369-89-1
Dithiocarbonic acid O-[(R)-1-((1R,2R)-2-hydroxy-1-methyl-cyclopentyl)-4-methyl-cyclohex-3-enylmethyl] ester S-methyl ester

: 84369-92-6
(R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene

Guidance literature:: Multi-step reaction with 3 steps

1: PPTS / CH₂Cl₂

2: LiAlH₄ / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00151a034

Reference yield:

: 84369-88-0
C₂₀H₂₄O₂S

: 84369-92-6
(R)-4-[(1S,2S)-2-(2-Ethoxy-ethoxy)-1-methyl-cyclopentyl]-1,4-dimethyl-cyclohexene

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) Li/NH₃, 2.) LiAlH₄ / 1.) THF, 30 min, reflux, 2.) Et₂O, 24 h, reflux

2: DBN / dimethylformamide / 0.25 h / 22 °C

3: PPTS / CH₂Cl₂

4: LiAlH₄ / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; 2,6-dichloro-benzonitrile; ammonia; pyridinium p-toluenesulfonate; lithium; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00151a034