tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylcarbamate

Base Information

• Chemical Name: tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylcarbamate
• CAS No.: 1069120-25-7
• Molecular Formula: C₂₃H₃₂N₂O₄S₂
• Molecular Weight: 464.65

Synonyms:tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylcarbamate

Chemical Property of tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylcarbamate

Chemical Property:

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Technology Process of tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylcarbamate

There total 1 articles about tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylthio)-3-methylbut-2-enyl)cyclohexylcarbamate (1069120-23-5) → tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylcarbamate (1069120-25-7)

Guidance literature:

With ammonium heptamolybdate dihydrate; dihydrogen peroxide; In ethanol; water; at 20 ℃; for 3h; Inert atmosphere;

DOI:10.1021/jm8006195

Reference yield:

tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylcarbamate (1069120-25-7) + trifluoroacetic acid (76-05-1) → (1S,4R)-4-((E)-4-(benzo[d]thiazol-2-ylsulfonyl)-3-methylbut-2-enyl)cyclohexylamine trifluoroacetate

Guidance literature:

In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/jm8006195

upstream raw materials:

tert-butyl-(1s,4s)-4-((E)-4-(benzo[d]thiazol-2-ylthio)-3-methylbut-2-enyl)cyclohexylcarbamate

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