<2α,3β(R)>-methyl 3-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-tetrahydro-5-oxo-1H-pyrrol-2-ylheptanoate

Base Information

• Chemical Name: <2α,3β(R)>-methyl 3-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-tetrahydro-5-oxo-1H-pyrrol-2-ylheptanoate
• CAS No.: 130584-65-5
• Molecular Formula: C₂₇H₄₅NO₆Si
• Molecular Weight: 507.743

Synonyms:<2α,3β(R)>-methyl 3-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-tetrahydro-5-oxo-1H-pyrrol-2-ylheptanoate

Chemical Property of <2α,3β(R)>-methyl 3-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-tetrahydro-5-oxo-1H-pyrrol-2-ylheptanoate

Chemical Property:

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Technology Process of <2α,3β(R)>-methyl 3-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-tetrahydro-5-oxo-1H-pyrrol-2-ylheptanoate

There total 1 articles about <2α,3β(R)>-methyl 3-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-tetrahydro-5-oxo-1H-pyrrol-2-ylheptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

<1α,2β(R)>-methyl 2-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-4-oxocyclobutylheptanoate (130584-61-1,130694-82-5) → <2α,3β(R)>-methyl 3-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-tetrahydro-5-oxo-1H-pyrrol-2-ylheptanoate (130584-65-5)

Guidance literature:

With N-hydroxy-2,4,6-trimethylbenzensulfonamide; In dichloromethane; at 20 ℃; for 5h;

Reference yield: 96.0%

<2α,3β(R)>-methyl 3-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-tetrahydro-5-oxo-1H-pyrrol-2-ylheptanoate (130584-65-5) → <2α,3β(R)>-methyl tetrahydro-3-(2-hydroxy-3-phenoxypropoxy)-5-oxo-1H-pyrrole-2-heptanoate (130584-66-6)

Guidance literature:

With hydrogen fluoride; In acetonitrile; 1) 0 - 5 deg C, 2) 20 deg C;

upstream raw materials:

<1α,2β(R)>-methyl 2-<2-(t-butyldimethylsilyloxy)-3-phenoxypropoxy>-4-oxocyclobutylheptanoate

Downstream raw materials:

<2α,3β(R)>-methyl tetrahydro-3-(2-hydroxy-3-phenoxypropoxy)-5-oxo-1H-pyrrole-2-heptanoate

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