C₂₁H₃₁BrFNO₅Si

Base Information

Chemical Name:C₂₁H₃₁BrFNO₅Si
CAS No.:1009092-79-8
Molecular Formula:C₂₁H₃₁BrFNO₅Si
Molecular Weight:504.469
Hs Code.:

C<sub>21</sub>H<sub>31</sub>BrFNO<sub>5</sub>Si

Synonyms:C₂₁H₃₁BrFNO₅Si

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Chemical Property of C₂₁H₃₁BrFNO₅Si

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Technology Process of C₂₁H₃₁BrFNO₅Si

There total 9 articles about C₂₁H₃₁BrFNO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1009092-77-6
C₈H₉BrFNO₂

: C₁₃H₂₆O₄Si

: 1009092-79-8
C₂₁H₃₁BrFNO₅Si

Guidance literature:: In toluene; Heating / reflux;

Reference yield:

: 874347-21-4
(S,Z)-5-(tert-butyldimethylsilyloxy)pent-3-en-2-ol

: 1009092-79-8
C₂₁H₃₁BrFNO₅Si

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / dmap / dichloromethane / 1 h / 0 - 20 °C

2: sodium iodide / acetone / 6 h / 20 °C

3: silver nitrate / acetonitrile / 6 h / 20 °C

4: sodium acetate / dimethyl sulfoxide / 0.5 h / 20 °C

5: toluene / Heating / reflux

With pyridine; sodium acetate; silver nitrate; sodium iodide; dmap; In dichloromethane; dimethyl sulfoxide; acetone; toluene; acetonitrile;

Reference yield:

: 147460-41-1
2-bromo-5-fluorophenol

: 1009092-79-8
C₂₁H₃₁BrFNO₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine; magnesium chloride / tetrahydrofuran / 0.17 h / 20 °C

1.2: 2 h / Heating / reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C

3.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

4.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

5.1: toluene / Heating / reflux

With hydrogenchloride; hydroxylamine hydrochloride; methyl orange; sodium cyanoborohydride; potassium carbonate; triethylamine; magnesium chloride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; toluene;