(((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane)

Base Information

• Chemical Name: (((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane)
• CAS No.: 1377359-03-9
• Molecular Formula: C₂₇H₄₈O₄SSi₂
• Molecular Weight: 524.913

Synonyms:(((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane)

Chemical Property of (((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane)

Chemical Property:

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Technology Process of (((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane)

There total 2 articles about (((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H30O4SSi (1290050-99-5) → (((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane) (1377359-03-9)

Guidance literature:

Multi-step reaction with 2 steps

1: tetrahydrofuran; toluene / 4 h / -10 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 1 h / Inert atmosphere

With triethylamine; In tetrahydrofuran; dichloromethane; toluene;

DOI:10.1021/jo300672a

Reference yield:

C21H34O4SSi + t-butyldimethylsiyl triflate (69739-34-0) → (((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane) (1377359-03-9)

Guidance literature:

With triethylamine; In dichloromethane; for 1h; Inert atmosphere;

DOI:10.1021/jo300672a

Reference yield: 76.0%

(((1S,2S,3S,4S)-2,4-dimethyl-6-methylene-5-(phenylsulfonyl)cyclohexane-1,3-diyl)bis(oxy))bis(tert-butyldimethylsilane) (1377359-03-9) → C21H44O2Si2 (1377359-05-1)

Guidance literature:

With sodium; In tetrahydrofuran; ethanol; at 0 - 20 ℃; for 8h; Inert atmosphere;

DOI:10.1021/jo300672a

upstream raw materials:

C₂₀H₃₀O₄SSi

t-butyldimethylsiyl triflate

Downstream raw materials:

C₂₁H₄₄O₂Si₂

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