N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide

Base Information

Chemical Name:N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide
CAS No.:710300-63-3
Molecular Formula:C₂₈H₄₄N₄O₇S₂
Molecular Weight:612.812
Hs Code.:

<i>N</i>-allyl-<i>N</i>-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide

Synonyms:N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide

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Chemical Property of N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide

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Technology Process of N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide

There total 7 articles about N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 106-95-6
allyl bromide

: 710300-60-0
N-((S)-2-Methyl-1-{[(S)-3-methyl-1-(piperidine-1-carbonyl)-butylsulfamoyl]-methyl}-propyl)-2-nitro-benzenesulfonamide

: 710300-63-3
N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 110-89-4
piperidine

: 710300-63-3
N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / BOP; DiPEA / CH₂Cl₂ / 1 h

2: 1.40 g / aq. HCl / CH₂Cl₂

3: N-methylmorpholine / CH₂Cl₂ / 1 h / 20 °C

4: Me₂NH / tetrahydrofuran; H₂O / 0.5 h / 20 °C

5: 1.71 g / Et₃N / CH₂Cl₂ / 20 °C

6: 87 percent / K₂CO₃ / dimethylformamide / 20 °C

With 4-methyl-morpholine; hydrogenchloride; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; dimethyl amine; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 710300-63-3
N-allyl-N-[1-({allyl-[3-methyl-1-(piperidine-1-carbonyl)-butyl]-sulfamoyl}-methyl)-2-methyl-propyl]-2-nitro-benzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: 100 percent / BOP; DiPEA / CH₂Cl₂ / 1 h

2: 1.40 g / aq. HCl / CH₂Cl₂

3: N-methylmorpholine / CH₂Cl₂ / 1 h / 20 °C

4: Me₂NH / tetrahydrofuran; H₂O / 0.5 h / 20 °C

5: 1.71 g / Et₃N / CH₂Cl₂ / 20 °C

6: 87 percent / K₂CO₃ / dimethylformamide / 20 °C

With 4-methyl-morpholine; hydrogenchloride; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; dimethyl amine; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;