3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid

Base Information

Chemical Name:3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid
CAS No.:864531-90-8
Molecular Formula:C₂₁H₂₄N₂O₇
Molecular Weight:416.431
Hs Code.:

3-(4-<i>tert</i>-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid

Synonyms:3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid

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Chemical Property of 3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid

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Technology Process of 3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid

There total 4 articles about 3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 71731-66-3
4-nitrobenzyl carbonazidate

: 4727-00-8,18822-59-8,186698-58-8
O-t-Butyl-L-tyrosine

: 864531-90-8
3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid

Guidance literature:: With sodium carbonate; In 1,4-dioxane; water; for 24h; pH=9 - 10;
DOI:10.1002/ejoc.200500167

Reference yield: 75.0%

: 71731-66-3
4-nitrobenzyl carbonazidate

: C₁₃H₁₉NO₃

: 864531-90-8
3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid

Guidance literature:: With sodium carbonate; In 1,4-dioxane; at 20 ℃; for 48h; pH=8 - 10;
DOI:10.1021/acs.joc.8b02553

Reference yield:

: 4457-32-3
4-nitrobenzyl chloroformate

: 864531-90-8
3-(4-tert-butoxy-phenyl)-2-(4-nitro-benzyloxycarbonylamino)-propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: NaN₃ / dioxane; H₂O / 2 h

2: 82 percent / Na₂CO₃ / dioxane; H₂O / 24 h / pH 9 - 10

With sodium azide; sodium carbonate; In 1,4-dioxane; water;
DOI:10.1002/ejoc.200500167