6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone

Base Information

Chemical Name:6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone
CAS No.:80602-07-9
Molecular Formula:C₁₄H₁₄N₂O
Molecular Weight:226.278
Hs Code.:

Synonyms:6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone

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Technology Process of 6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone

There total 3 articles about 6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: dimethyloxosulfonium acetyl (6-methyl-2-phenyl-4-pyrimidinyl)methylide

: 80602-07-9
6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone

Guidance literature:: With deactivated Raney nickel; In methanol; for 0.5h; Heating;

Reference yield:

: 80601-96-3
dimethyloxosulfonium 6-methyl-2-phenyl-4-pyrimidinylmethylide

: 80602-07-9
6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / dioxane / 1 h / Ambient temperature

2: 88 percent / deactivated Raney nickel / methanol / 0.5 h / Heating

With deactivated Raney nickel; In 1,4-dioxane; methanol;

Reference yield:

: 29509-92-0
4-chloro-6-methyl-2-phenyl-pyrimidine

: 80602-07-9
6-methyl-2-phenyl-4-pyrimidinylmethyl methyl ketone

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / tetrahydrofuran / 5 h / Heating

2: 88 percent / dioxane / 1 h / Ambient temperature

3: 88 percent / deactivated Raney nickel / methanol / 0.5 h / Heating

With deactivated Raney nickel; In tetrahydrofuran; 1,4-dioxane; methanol;